Related Products of 5969-83-5, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 5969-83-5, name is 2-(4-Chlorophenyl)pyridine. This compound has unique chemical properties. The synthetic route is as follows.
General procedure: In a typical reaction, a 10 mL oven-dried reaction vessel was charged with Pd/MgLa mixed oxide (30 mg), 2-phenylpyridine (29 mg, 0.2 mmol), benzyl alcohol (108 mg, 1 mmol), tert-butyl hydroperoxide (70% solution in water, ?129 mg, 1 mmol) and chlorobenzene (0.5 mL) were added. The resulting solution was stirred at 120 C for 8 h in open air. The reaction was monitored by thin-layer chromatography (TLC). After cooling to room temperature, catalyst was separated by simple centrifugation. The filtrate was concentrated under reduced pressure and the residue was purified by column chromatography using silica gel and a mixture of hexane/ethyl acetate as eluents. All the products were confirmed by 1H NMR and 13C NMR spectroscopy. The recovered catalyst was used for the next cycle without any further purification.
According to the analysis of related databases, 5969-83-5, the application of this compound in the production field has become more and more popular.
Reference:
Article; Kishore; Kantam, M. Lakshmi; Yadav; Sudhakar; Laha; Venugopal; Journal of Molecular Catalysis A: Chemical; vol. 379; (2013); p. 213 – 218;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem