Category: 65753-52-8

As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 65753-52-8, name is 2-Fluoro-3-(trifluoromethyl)pyridine, molecular formula is C6H3F4N, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. name: 2-Fluoro-3-(trifluoromethyl)pyridine

750 g of 2-fluoro-3-trifluoromethylpyridine was added to the ammoniation reactor.700g of water was added to the ammoniation reactor, and then 250g of liquid ammonia was fed to the ammoniation reactor.Raise temperature to 130C, pressure not more than 3.0MPa, react for 10 hours,Cool down to 90 C, discharge to the receiving kettle, receive cooling down to 10 C,2-Amino-3-trifluoromethylpyridine is obtained by centrifugation and drying; the yield is about 95%

With the rapid development of chemical substances, we look forward to future research findings about 65753-52-8.

Reference:
Patent; Shandong Huimeng Biological Technology Co., Ltd.; Xiao Caigen; Liu Shuwen; (6 pag.)CN108003093; (2018); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem

As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 65753-52-8, name is 2-Fluoro-3-(trifluoromethyl)pyridine, molecular formula is C6H3F4N, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. name: 2-Fluoro-3-(trifluoromethyl)pyridine

750 g of 2-fluoro-3-trifluoromethylpyridine was added to the ammoniation reactor.700g of water was added to the ammoniation reactor, and then 250g of liquid ammonia was fed to the ammoniation reactor.Raise temperature to 130C, pressure not more than 3.0MPa, react for 10 hours,Cool down to 90 C, discharge to the receiving kettle, receive cooling down to 10 C,2-Amino-3-trifluoromethylpyridine is obtained by centrifugation and drying; the yield is about 95%

With the rapid development of chemical substances, we look forward to future research findings about 65753-52-8.

Reference:
Patent; Shandong Huimeng Biological Technology Co., Ltd.; Xiao Caigen; Liu Shuwen; (6 pag.)CN108003093; (2018); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem

As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 65753-52-8, name is 2-Fluoro-3-(trifluoromethyl)pyridine, molecular formula is C6H3F4N, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. name: 2-Fluoro-3-(trifluoromethyl)pyridine

750 g of 2-fluoro-3-trifluoromethylpyridine was added to the ammoniation reactor.700g of water was added to the ammoniation reactor, and then 250g of liquid ammonia was fed to the ammoniation reactor.Raise temperature to 130C, pressure not more than 3.0MPa, react for 10 hours,Cool down to 90 C, discharge to the receiving kettle, receive cooling down to 10 C,2-Amino-3-trifluoromethylpyridine is obtained by centrifugation and drying; the yield is about 95%

With the rapid development of chemical substances, we look forward to future research findings about 65753-52-8.

Reference:
Patent; Shandong Huimeng Biological Technology Co., Ltd.; Xiao Caigen; Liu Shuwen; (6 pag.)CN108003093; (2018); A;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem