Adding a certain compound to certain chemical reactions, such as: 170165-79-4, 1,3-Di(pyridin-4-yl)benzene, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Quality Control of 1,3-Di(pyridin-4-yl)benzene, blongs to pyridine-derivatives compound. Quality Control of 1,3-Di(pyridin-4-yl)benzene
General procedure: A mixture of Zn(NO3)2 (0.15 mmol), 1,3-dpb and glu2- (0.1 mmol) was dissolved in 8 ml of DMF-MeOH-H2O (1 : 1 : 2, v/v). The final mixture was placed in a Parr Teflon-lined stainless steel vessel (15 ml) and heated at 110 C for3 days, colourless crystals were obtained (52% yield based on 1,3-dpb). IR (KBr, gamma/cm-1): 3425 (m), 3068 (w), 2848 (w), 2359 (m), 1580 (s), 1515 (s), 1394 (s), 1226 (s), 1156 (w), 1056 (s), 964 (w), 852 (w), 757 (m), 674 (m), 536 (m). Found (%): C, 59.06; H, 4.13; N, 6.41. Calc. for C21H18N2O4Zn (%): C, 58.96; H, 4.24; N, 6.55.
The synthetic route of 170165-79-4 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Hu, Jin-Song; Lei, Zhang; Xing, Hong-Long; Zhang, Xiao-Mei; Shi, Jian-Jun; He, Jie; Mendeleev Communications; vol. 23; 4; (2013); p. 229 – 230;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem